Acta Crystallographica Section E: Structure Reports Online - Volume 68, issue Pt 1

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Electronic ISSN
1600-5368

Abstract

The crystal of the title compound, C21H23NO2, was chosen from a conglomerate formed by a racemic mixture. An intra­molecular hydrogen bond is formed between hy­droxy group and heterocyclic N atom of the aza­bicyclo­[3.2.1]octan-3-one system. The crystal structure

Abstract

In the title compound [systematic name: 7,8-dimeth­oxy-11-methyl-17,19-dioxa-11-aza­tetra­cyclo­[12.7.0.04,9.016,20]henicosa-1(21),4,6,8,14,16 (20)-hexaen-2-ol], C21H25NO5, the benzene rings are inclined at a dihedral angle of 23.16 (5)°. One

Abstract

In the title compound, C11H12N4S, the thio­phene ring is roughly planar, with a maximum deviation of 0.012 (1) Å for the S atom, and makes a dihedral angle of 7.89 (8)° with the mean plane of the piperidine ring, which is in a chair conformation. The crystal packi

Abstract

In the title compound, C19H15Cl2N3O2, the benzotriazole ring system is approximately planar [maximum deviation = 0.018 (2) Å] and its mean plane is oriented at dihedral angles of 30.70 (5) and 87.38 (4)°, respectively, to the furan and benzen

Abstract

In the title compound, C11H8O3S2, the dihedral angle between the mean planes of the two thio­phene rings is 65.10 (10)°. Intra­molecular C—H⋯O inter­actions form S(6) and S(7) ring motifs. In the crystal, chains along the a axis are

Abstract

The structure of the title compound, [Mn(NCS)2(C6H8N2)4], consists of isolated mol­ecules of [Mn(NCS)2(Aim)4] (Aim = 1-allyl­imidazole), which contain a compressed octa­hedral MnN6 chromophore (site symmetry )

Abstract

In the crystal structure of the title compound, C15H20N2O3S, the hy­droxy group is involved in the formation of O—H⋯N hydrogen bonds, which link two mol­ecules into a centrosymmetric dimer. Weak C—H⋯O hydrogen bonds further link these dimers into chains

Abstract

The title compound, C9H13Br2ClNTe, was synthesized by reacting [2-(dimethyl­amino­meth­yl)phen­yl]tellurium(II) chlor­ide with Br2. As a consequence, the Cl and Br atoms are not well ordered but distributed over the three possible positions such that th

Abstract

The dimethoxypbenzene ring in the title compound, C19H21NO5, is gauche to the amide group and anti to the ester group. The chirality was confirmed to be S from two-dimensional NMR spectroscopy. In the crystal, N—H⋯O and C—H⋯O hydrogen bonds an

Abstract

In the title mol­ecule, C26H22P2Se2, both P atoms have distorted tetra­hedral environments, resulting in effective cone angles of 177 and 174°. Inversion twinning was detected and refined to a ratio of 0.35:0.65. Weak inter­molecular C—H⋯Se inter­action