Acta Crystallographica Section E: Structure Reports Online - Volume 67, issue Pt 6

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Electronic ISSN
1600-5368

Abstract

The title compound, C34H40N2O4·2C3H7NO, was synthesized by the Mannich condensation of ethane­diamine, formaldehyde and p-cresol. In the crystal, the tetra­phenol mol­ecule is arranged around an inversion center. The mol­ecu

Abstract

In the title solvated mol­ecular salt, C28H28NO+·Cl·C2H4O2, the central piperidinium ring of the cation adopts an envelope conformation with the N atom displaced by 0.798 (2) Å from the mean plane of the five C atoms. I

Abstract

In the title compound, C18H17FO2S, the 3-fluoro­phenyl ring makes a dihedral angle of 78.30 (5)° with the mean plane of the benzofuran fragment. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O hydrogen bonds and C—H⋯π inter­actions.

Abstract

The title compound, [Pb4(C8H4O4)3Cl2]n, consists of a three-dimensional inorganic–organic hybrid framework. The asymmetric unit contains two Pb2+ cations, one Cl anion and one and a half ter

Abstract

In the title compound, 2C2H8NO+·C14H8O42−, the dihedral angle between the benzene rings of the dianion is 9.95 (12)°. In the crystal, the cations and anions are linked via inter­molecular O—H⋯O and N—H⋯O hydrogen

Abstract

The acetonitrile ligand in the title compound, [W(CH3CN)(CO)5], is coordinated end-on to a penta­carbonyl­tungsten(0) fragment with a W—N bond length of 2.186 (4) Å, completing an octa­hedral coordination environment around the W atom.

Abstract

The MnIII atom in the title complex, [Mn(C18H18N2O4)(CHO2)(H2O)]·2H2O, is O,N,N′,O′-chelated by the deproton­ated Schiff base; the four chelating atoms form an approximate square, w

Abstract

In the title compound, C18H18O2S, the phenyl ring makes a dihedral angle of 87.47 (6)° with the mean plane of the benzofuran fragment. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O hydrogen bonds and C—H⋯π inter­actions.

Abstract

In the title compound, C27H24N2O·0.7H2O, the quinoline ring system is approximately planar, with a maximum deviation of 0.011 (1) Å, and forms dihedral angles of 74.70 (4) and 80.14 (4)° with the phenyl and benzene rings, respectively. In the crystal, t

Abstract

The title compound, C7H6O5·H2O, is a new polymorph of the structures reported by Jiang et al. (2000 ▶) [Acta Cryst. C56, 594–595] and Okabe et al. (2001 ▶) [Acta Cryst. E57, o764–o766]. The gallic acid mol­ecule