Acta Crystallographica Section E: Structure Reports Online - Volume 67, issue Pt 11

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Electronic ISSN
1600-5368

Abstract

The title compound, C14H10F3NO3, was prepared by a palladium-catalysed Suzuki–Miyaura coupling reaction. The dihedral angle between the nitro group and its parent benzene ring is 66.85 (19)° while the dihedral angle between the two benzene rings is 49.9

Abstract

In the title compound, [ZnBr2(C12H9N3O2)], the ZnII ion is bonded to two Br ions and two N atoms of the diimine ligand in a distorted tetra­hedral geometry. With the exception of the Br atoms, all other atoms are disordered over tw

Abstract

The title compound, C14H8N6O12, is centrosymmetric, the mid-point of the central C—C bond being located on an inversion centre. Two of the three independent nitro groups are disordered over two sites, with a site-occupancy ratio of 0.513 (3):0.487 (3).

Abstract

The title compound, C13H13FO3S, was prepared by alkaline hydrolysis of ethyl 2-(5-fluoro-3-isopropyl­sulfanyl-1-benzofuran-2-yl)acetate. In the crystal, the carb­oxy groups are involved in inter­molecular O—H⋯O hydrogen bonds, which link the mol­ecules into centro

Abstract

In the title polymeric compound, [Cd(C9H12O4)(C10H8N2)]n, the CdII atom is located on a twofold rotation axis and is coordinated by two 4,4′-bipyridine ligands and two 2,2-dimethyl­cyclo­pentane-1,3-dic

Abstract

In the title compound, [AuCl(C25H23N2P)], the AuI atom is in a typical almost linear coordination environment defined by phosphane P and Cl atoms [bond angle = 175.48 (4)°]. Helical supra­molecular chains along the b axis and mediated by N—H⋯Cl h

Abstract

The title compound, C11H15BrNO+·Cl, was obtained as a precursor within our current program for the synthesis of new β-amino­alcohols via a Mannich-type reaction. The protonated amino N atom is hydrogen bonded to the chloride anion. With exceptio

Abstract

In the title compound, C20H21N3, the pyrimidine ring is inclined at dihedral angles of 51.57 (4) and 2.49 (4)° to the two phenyl rings. The dihedral angle between the two terminal phenyl rings is 50.44 (4)°. In the crystal, adjacent mol­ecules are linked via

Abstract

The asymmetric unit of the title compound, C14H10N4O2, contains two independent mol­ecules with similar structures. In one mol­ecule, the tetra­zole ring is oriented at dihedral angles of 17.71 (16) and 57.13 (17)°, respectively, to the central benzene