Acta Crystallographica Section E: Structure Reports Online - Volume 66, issue Pt 7

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Electronic ISSN
1600-5368

Abstract

In the title compound, C8H9ClN2O3S, the benzene ring makes a dihedral angle of 4.1 (9)° with the amido –NHCO– plane including the major occupancy component of the carbonyl O atom [19 (4)° for the minor component]. An intra­molecular C—H⋯O inter­action o

Abstract

In the title compound, C14H13NO3S, the conformation of the N—H bond in the C—SO2—NH—C(O) segment is anti to the C=O bond. The dihedral angle between the sulfonyl benzene ring and the S—N—C—O segment (r.m.s. deviation = 0.039 Å) is 77.1 (1)° and t

Abstract

In the title mononuclear iron(III) complex, [Fe(C15H13N2O3)2]Cl·H2O, the FeIII atom has a distorted octa­hedral geometry and is six-coordinated by four O atoms and two N atoms from two ligands. In the crystal structure,

Abstract

In the title compound, C15H13FO3, the dihedral angle between the two aromatic rings is 52.78 (8)°. In the crystal, inter­molecular C—H⋯O hydrogen bonds link mol­ecules into chains running parallel to the c axis.

Abstract

The structure of the title compound, C13H17NO, features an anti disposition of the N—H and carbonyl groups. The amide group is twisted with respect to the benzene ring [N–C(=O)–C–C torsion angle = −30.8 (4)°]. In the crystal, C(4) chains propagating in [100] ar

Abstract

In the title compound, C23H26O, the adamantane cage consists of three fused cyclo­hexane rings in classical chair conformations with absolute values of the C—C—C angles in the range 106.57 (11)–111.56 (12)°. The dihedral angle between the two phenyl rings is 81.38 (4)°. Alth

Abstract

In the title compound, C18H24N4O·H2O, the piperizine ring adopts a chair conformation and the dihedral angle between the phenyl and pyridine rings is 39.9 (3)°. The comformations of the attachment of the anisole and N-ethyl­pyridin-2-amine groups

Abstract

The quinter­nary thio­phosphate Cs0.5Ag0.5Nb2PS10, cesium silver tris­(disulfido)[tetra­thio­phosphato(V)]diniobate(IV), has been prepared from the elements using a CsCl flux. The crystal structure is made up of 1[Nb2PS

Abstract

Cocrystallization of benzimidazole with benzene 1,3,5-tricarb­oxy­lic acid in slightly basic medium afforded the title compound, C7H7N2+·C9H5O6·3H2O, in which one of the imidazole N atom is protona