Acta Crystallographica Section E: Structure Reports Online - Volume 65, issue Pt 11

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Electronic ISSN
1600-5368

Abstract

The asymmetric unit of the title compound, C12H13NO3, contains two independent mol­ecules. The conformation of the N—H bond and the C=O bond in the amide segment are anti to each other. The mol­ecular conformation of each mol­ecule is stabilized by an intra

Abstract

The title compound, C7H4BrNO3, was isolated as a by-product while attempting to prepare a diselenide. There is a close intra­molecular Br⋯O contact [2.984 (2) Å]. The mol­ecules form loosely associated dimers held together by weak inter­molecular Br⋯O inter­action

Abstract

The title compound, [NH3(CH2)2NH3][Mg(SO4)2(H2O)4], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetra­aqua­bis(sulfato

Abstract

The title compound, [Ti(C10H15)(C20H26Si)], was obtained from the reaction of [Ti{η51-C5Me4(CH2)}(η5-C5Me5)] with the alkynylsilane PhC2SiMe2

Abstract

The title dinuclear copper complex, [Cu2(C15H15N6O)Cl2(CH3OH)2]ClO4, was prepared by the reaction of copper(II) chloride with bis­[1-(2-pyrid­yl)ethyl­idene]carbonohydrazide in the presence of sodium perchlora

Abstract

In the title compound, C18H13ClN2OS, the thia­zolidinone ring is slightly distorted and adopts a envelope conformation. The basal plane is nearly perpendicular to the quinoline ring, forming a dihedral angle of 86.1 (1)°, and makes a dihedral angle of 14.9 (1)° to

Abstract

In the title compound, C12H16N2O4, an intra­molecular O—H⋯O hydrogen bond occurs. In the crystal, mol­ecules are linked by N—H⋯O hydrogen bonds, forming chains propagating in the [010] direction.

Abstract

The structure of the title compound, C14H12O2, resembles those of phenyl benzoate and 4-methyl­phenyl benzoate, with similar bond parameters. The two aromatic rings make a dihedral angle of 76.0 (1)°. The plane of the central —C(=O)—O— group is twisted by 9.4 (2)°

Abstract

In the crystal structure of the title salt, C8H11N4O2+·C6H2N3O7, the pictrate anion participates in extensive hydrogen bonding with the guanidinium ion group of the cation, linking the m

Abstract

In the title compound, C15H10F2O2S, the O atom and the methyl group of the methyl­sulfinyl substituent lie on opposite sides of the plane through the benzofuran fragment. The 4-fluoro­phenyl ring is rotated out of the benzofuran plane by a dihedral angl